By André Gourdon
With contributions via prime overseas specialists, this e-book offers a close compilation of a brand new and intensely lively box. it's the first ebook dedicated to the covalent coupling of molecular precursors on surfaces that enables the training of 0D, 1D and 2nd molecules that can't be synthesized in resolution. This booklet is aimed toward scholars and researchers attracted to nanochemistry and molecular units and it supplies the reader a pedagogical up to date imaginative and prescient of the latest advancements. The editor guarantees a multidisciplinary process related to molecular chemistry, floor sciences, floor spectroscopies, thought, scanning tunneling and non-contact atomic strength microscopies.
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Additional resources for On-Surface Synthesis: Proceedings of the International Workshop On-Surface Synthesis, École des Houches, Les Houches 25-30 May 2014
1). The idea is to use molecular precursors to build-up complex nanostructures that can range from purely 2D organic layers, networks or templates, to 1D nanowires or zero-dimensional (0D) nanoobjects. In this outlined picture, the ﬁrst step is to obtain the desired molecular bricks or reagents. Thus, the desired precursor, represented in Fig. 1 by reddish spheres, is usually synthesized with a molecular connector at the borders (small yellow ball in Fig. 1). These linkers, connectors or end-groups stabilize the molecule termination and they could be halide elements, methyl, amine groups or simply hydrogen atoms.
Chem. Eur. J. 20, 4111 (2014) 28. : Efﬁcient, selective, and recyclable palladium catalysts in carbon-carbon coupling reactions. Chem. Rev. 111, 2251 (2011) 29. : Carbon-carbon coupling reactions catalyzed by heterogeneous palladium catalysts. Chem. Rev. 107, 133 (2007) 30. : An ab initio insight into the Cu(111)-mediated Ullmann reaction. Phys. Chem. Chem. Phys. 13, 154 (2011) 31. : Effect of substituents on the phenyl coupling reaction on Cu (111). Surf. Sci. 337, 40 (1995) 32. : Combined scanning tunneling microscopy and kinetic Monte Carlo study on kinetics of Cu-coordinated pyridyl-porphyrin supramolecular self-assembly on a Au(111) surface.
Further annealing at 430 K led to irregular polymer network structures associated with the molecules fully converted to the FS (Fig. 4e). Differing from the Cu(111) case, we did not observe any IntS on the Au(111) surface in the temperature range between 300 and 450 K. Walch et al.  reported that molecules 2 keep intact on Ag(111) surface at room temperature. Here, we examined its high-temperature behavior. As shown in Fig. 4g, after an annealing at 390 K, an open network structure consisting of polygons replaced the close-packed molecular monolayer formed at room temperature.